| 甲苯(mL) | 水(mL) | 正丁醇(mL) | 温度(℃) | TMP(g) | 二水合氯化铜(g) | 盐酸羟胺(g) | 氯化锂(g) | Et2NH2Cl(g) | 六水合氯化铁(g) | 时间 | 收率% |
| 25 | 25 | 25 | 60 | 3 | 0.76 | 0.75 | 4 h | 58.63 | |||
| 25 | 25 | 25 | 60 | 3 | 0.76 | 0.93 | 4 h | 62.06 | |||
| 25 | 25 | 25 | 80 | 3 | 0.76 | 1.02 | 2 h | 70.87 | |||
| 25 | 25 | 25 | 70 | 3 | 3.36 | 3.74 | 2 h | 65.31 | |||
| 25 | 25 | 25 | 70 | 3 | 0.76 | 1.2 | 4 h | 15.23 | |||
| 25 | 25 | 25 | 60 | 3 | 0.76 | 0.5 | 5 h | 5.31 | |||
| 25 | 25 | 25 | 70 | 3 | 0.76 | 1.2 | 4 h | 19.77 | |||
| 35 | 25 | 15 | 70 | 3 | 0.76 | 0.78 | 3 h | 25.38 | |||
| 0 | 0 | 50 | 70 | 3 | 0.76 | 0.78 | 2 h | 25.30 | |||
| 0 | 0 | 50 | 60 | 3 | 0.76 | 0.78 | 4 h | 72.09 | |||
| 0 | 0 | 50 | 40 | 3 | 0.76 | 0.78 | 5 h | 76.15 | |||
| 0 | 0 | 50 | 40 | 3 | 0.76 | 0.78 | 4 h | 76.45 | |||
| 0 | 0 | 50 | 65 | 3 | 0.76 | 0.78 | 2 h | 83.16 | |||
| 0 | 0 | 50 | 60 | 3 | 0.76 | 0.78 | 2 h | 83.17 | |||
| 0 | 0 | 50 | 50 | 3 | 0.76 | 0.78 | 3 h | 81.78 | |||
| 10 | 0 | 40 | 60 | 3 | 0.76 | 0.78 | 3 h | 85.38 | |||
| 甲醇(mL) | |||||||||||
| 0 | 0 | 50 | 60 | 3 | 0.76 | 0.78 | 3 h | 83.43 | |||
| 25 | 0 | 25 | 60 | 3 | 0.76 | 0.50 | 2 h | 81.52 | |||
| 25 | 0 | 25 | 60 | 3 | 1.5 | 2.5 | 4 h | 杂质明显 | |||
| 25 | 0 | 25 | 60 | 3 | 0.8 | 1.3 | 4 h | 杂质明显 |